Ethanol solutions in D 2 O were initially prepared (5%, 10%, 15%, 20%, 25%, 30% v/v), and then, 0.6 mL of each solution was transferred separately to an NMR tube, and finally inserted into the NMReady ...

The NMR tube is filled with exactly 500µL of 1- octanol, capped, and inverted for 15-20 times for thorough mixing. The layers are then allowed to separate for roughly 5min. ... The 1 H NMR spectrum of ...