This project leverages the unique high-temperature and –pressure MAS NMR technology at the Pacific Northwest National Laboratory (PNNL). Using the 13C labeled lignin model polymers at different ...

Examples of one–dimensional 13 C magic–angle spinning (MAS) NMR spectra of sample 2 are shown in Fig. 1 . In the absence of Fab (Fig. 1a), ...

Two-dimensional (2D) 1H-13C methyl correlated NMR is increasingly being recognized as a powerful tool to characterize the higher order structure (HOS) of monoclonal antibody (mAb) therapeutics. 2D ...

In this study, the researchers utilized an innovative solid-state NMR method: 1 H-13 C Frequency Switched Lee Goldburg Heteronuclear Correlation (FSLG-HETCOR) NMR. By optimizing key parameters such as ...

An example of one MAS NMR spectrum. This is used to identify atoms in the molecule and, ultimately, for calculating their 3-D structures.

Most often, 13 C NMR spectroscopy is used, but many other nuclei (e.g., 19 F, 15 N, 23 Na, 31 P, 17 O, or 2 H) can be used, depending on what will be studied. NMR spectroscopy is unique because it can ...

This webinar introduces the fundamental aspects of FAST MAS SSNMR and demonstrates useful applications of such a high-spinning regime (≥ 40 kHz) for pharmaceutical systems. Due to the considerable ...

UK NMR facility orders Europe's first 1 mm magic-angle spinning probe November 10th, 2011 The National Management Committee of the UK 850 MHz Solid-State NMR facility, based at the University of ...