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Learn how to interpret ¹H and ¹³C NMR spectroscopy results with this beginner-friendly guide. Understand chemical shifts, splitting patterns, integration, and structural analysis techniques.
A well-configured solution is essential to completing solid-state NMR experiments effectively. The magic angle setting is a crucial factor in a magic angle spinning (MAS) probe, pivotal for achieving ...
We will discuss NMR applications in the field in the last 10 years, recent advances in NMR instrumentation, and explore important features in data analysis. However, while this work aims to serve as a ...
In this article, Bruker BioSpin explains everything there is to know about carbon dioxide/carbonate processes in aqueous solution.
We have thus developed a quantitative magic-angle spinning (MAS) 13 C NMR approach coupled with cross-polarization (CP) and/or Insensitive Nuclei Enhanced by Polarization Transfer (INEPT) on rigid and ...
This work describes a method to predict the 125Te and 13C NMR chemical shifts of diorgano tellurides based in a three-dimensional approach. For that, a collection of 150 compounds were selected from ...
13 C– 13 C 2D correlations were measured using 20 ms DARR mixing with the 1 H amplitude at the MAS frequency. A total of 280 complex t1 points with increment of 25 μs were recorded. For 13 C- 15 N 1D ...
In this study, we have synthesized 13C labeled lignin model polymers with only β-O-4 linkages and hydroxyphenyl monomers of different molecular weights to perform in-situ magic angle spinning (MAS) ...